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injektorbetingelserne justeres (temperatur, splitforhold og injektionsvolumen), så sondringen mellem palmitinsyre og palmitolsyre minimeres.
adjust the injector conditions (temperature, split ratio and volume injection) to minimise the discrimination of palmitic and palmitoleic acid.
driftsbetingelser: bæregas: brint eller helium- bæregasflow: ca. 2 ml/min.- injektor- og detektortemperatur: 300° c- temperaturprogrammering: 1 minut ved 160° c, 4° c/minut, indtil 260°c, derefter konstant temperatur ved 260°c i 15 min.- splitforhold: ca. 1:20.
operating conditions:- carrier gas: hydrogen or helium,- carrier gas flow rate: about 2 ml/minute,- injector and detector temperature: 300 °c,- programming of temperature: 1 minute at 160 °c, 4 °c per minute to 260 °c, constant temperature of 260 °c for 15 minutes,- splitter ratio: about 1:20.