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niiskuse imendumist (märkus 6) vältides lisatakse alkoholifraktsiooni sisaldavasse katseklaasi iga alkoholi milligrammi kohta 50 l silüülivat reagenti, mis koosneb 9 : 3 : 1 mahuga (märkus 5) püridiin-heksametüüldisilasaan-trimetüülklorosilaani segust.
the reagent for silylation, consisting of a mixture of 9:3:1 by volume (note 5) of pyridinehexamethyldisilazane-trimethylchlorosilane in the proportion of 50 ml for each milligram of alcohols, is added to the test tube containing the alcoholic fraction, avoiding all absorption of moisture (note 6).