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lc-ms : m+h = 422 pf (°c) : 129-130°c rmn x h (cdc1 3 ) δ(ppm) : 2,95 (d, 3h) ; 3,20-3,35 (m, 4h) ; 3 , 65-3 , 80 (m, 4h) ; 4 , 65 ( s , 2h) ; 6 , 05 ( large s , 1h) ; 7 , 05 (d, 2h) ; 7 , 50-7 , 60 (m, 4h) ; 7 , 65-7 , 80 (m, 2h) exemple 3 (composé n°76) 4-{5- [3- (trifluorornéthyl)phényl] -2-pyridinyl}-l- pipérazinecarboxylate de 2- (méthylamino) -2-oxoéthyle 3.1.
lc-ms: m+h=422 m.p. (° c.): 129-130° c. 1 h nmr (cdcl 3 ) δ (ppm): 2.95 (d, 3h); 3.20-3.35 (m, 4h); 3.65-3.80 (m, 4h); 4.65 (s, 2h); 6.05 (broad s, 1h); 7.05 (d, 2h); 7.50-7.60 (m, 4h); 7.65-7.80 (m, 2h) example 3 compound 76 2-(methylamino)-2-oxoethyl 4-{5-[3-(trifluoromethyl)-phenyl]-2-pyridyl}-1-piperazinecarboxylate 3.1.
Last Update: 2014-12-03
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