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ak titer pre druhý destilát je viac ako 2 ml, opakujte test a začnite destiláciu znovu s použitím čerstvého podielu lúhovacieho roztoku.
if the titre for the second distillate is more than 0,2 ml, repeat the test and start the distillation again using a fresh aliquot of digest solution.
ak je titer druhého destilátu viac ako 0,2 ml, opakujte skúšku a znovu začnite destiláciu, pričom použite čerstvý alikvótny podiel lúhovacieho roztoku.
if the titre for the second distillate is more than 0,2 ml, repeat the test and start the distillation again using a fresh aliquot of digest solution.
do destilačnej banky premiestnite presne 10 ml lúhovacieho roztoku, do lievika pridajte nie menej ako 5 ml roztoku hydroxidu sodného, zľahka zdvihnite zátku a nechajte roztok hydroxidu sodného pomaly natekať do banky.
transfer exactly 10 ml of digest solution to the distillation flask, add not less than 5 ml of sodium hydroxide solution to the funnel, lift the stopper slightly and allow the sodium hydroxide solution to run slowly into the flask.
banku nechajte ochladiť, opatrne rozrieďte obsah 10 – 20 ml vody, ochlaďte, preneste obsah kvantitatívne do 200 ml odmernej banky a doplňte objem vodou na vytvorenie lúhovacieho roztoku.
allow the flask to cool, dilute the contents carefully with 10 — 20 ml water, cool, transfer the contents quantitatively to a 200 ml graduated flask and make up to volume with water to form the digest solution.
do destilačnej banky prelejte presne 10 ml lúhovacieho roztoku, do lievika pridajte najmenej 5 ml roztoku hydroxidu sodného, mierne zdvihnite zátku a nechajte roztok hydroxidu sodného pomaly natekať do banky.
transfer exactly 10 ml of digest solution to the distillation flask, add not less than 5 ml of sodium hydroxide solution to the funnel, lift the stopper slightly and allow the sodium hydroxide solution to run slowly into the flask.