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10 mg of imidazole and 70 mg of methylphenylphosphinic chloride are added.
10 mg d'imidazole et 70 mg de chlorure methylphenylphosphinique sont ajoutés.
Last Update: 2014-12-03
Usage Frequency: 1
Quality:
995 mg of methylphenylphosphinic acid 4-nitrophenyl ester are obtained with a purity of 50%.
995 mg de methyl-phenyl-phosphinic acid 4-nitro-phenyl ester sont obtenus avec une pureté de 50 %.
Last Update: 2014-12-03
Usage Frequency: 1
Quality:
after stirring for approximately one hour, 5.76 mg of imidazole and 20.7 mg of methylphenylphosphinic chloride are added.
après environ une heure d'agitation 5.76 mg d'imidazole et 20.7 mg de chlorure methylphenylphosphinique sont ajoutés.
Last Update: 2014-12-03
Usage Frequency: 1
Quality:
after stirring for approximately 1 hour at ambient temperature, a solution of 630 mg of methylphenylphosphinic chloride in 2 ml of anhydrous tetrahydrofuran is added dropwise over about ten minutes.
après environ 1 heure d'agitation à température ambiante, une solution de 630 mg de chlorure méthylphenylphosphinique dans 2 ml de tetrahydrofurane anhydre est additionnée goutte à goutte en une dizaine de minutes.
Last Update: 2014-12-03
Usage Frequency: 1
Quality:
after stirring for 15 hours, a further 16 mg of imidazole and 40.5 mg of methylphenylphosphinic chloride are added and the mixture is stirred at ambient temperature for another 3½ hours in order for the reaction to be complete.
après 15 heures d'agitation ajoute à nouveau 16 mg d'imidazole et 40.5 mg de chlorure methylphenylphosphinique et agite à température ambiante encore 3.5 heures pour que la réaction soit complète.
Last Update: 2014-12-03
Usage Frequency: 1
Quality:
16 mg of imidazole and 40.5 mg of methylphenylphosphinic chloride are added to a solution of 27 mg of 3-[1-tert-butoxycarbonyl-5-(2-morpholin-4-yl-ethoxy)-1h-indol-2-yl]-5-hydroxyindazole-1-carboxylic acid tert-butyl ester in 2 ml of dichloromethane.
a une solution de 27 mg de 3-[1-tert-butoxycarbonyl-5-(2-morpholin-4-yl- ethoxy)-1 h-indol-2-yl]-5-hydroxy-indazole-1 -carboxylic acid tert-butyl ester dans 2 ml de dichloromethane est ajouté 16 mg d'imidazole et 40.5 mg de chlorure methylphenylphosphinique.
Last Update: 2014-12-03
Usage Frequency: 1
Quality: