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calibration involves heating a tube (fitted with a 1.5 mm orifice plate) filled with 27 cm3 of dibutyl phthalate. the time taken for the temperature of the liquid (measured with a 1 mm diameter thermocouple centrally placed 43 mm below the rim of the tube) to rise from 50 °c to 250 °c is recorded and the heating rate calculated.
校准程序包括加热一根装有27立方厘米邻苯二甲酸二丁酯的钢管(配有一块带1.5毫米圆孔的板)，记录液体温度(用放在钢管中央距离管口43毫米处的直径1毫米热电偶测量)从50℃上升至250℃所需的时间，然后计算加热速度。