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gleichzeitig verringert sich der nicht umgesetzte mdu-anteil.
at the same time the proportion of unreacted mdu decreased.
Última atualização: 2014-12-03
Frequência de uso: 2
Qualidade:
es werden jeweils 600 g mdu-lösung und 48,3 g erfindungsgemäßer katalysator eingesetzt.
in each case there were used 600 g of mdu solution and 48.3 g of inventive catalyst.
Última atualização: 2014-12-03
Frequência de uso: 4
Qualidade:
wenn ein anderer mdu- und/oder n-butanolgehalt gewünscht wird, werden die eduktmengen entsprechend angepasst.
when a different mdu and/or n-butane content was desired, the quantities of starting materials were adapted accordingly.
Última atualização: 2014-12-03
Frequência de uso: 2
Qualidade:
die verbleibenden 628,7 g/h bis-(4-butoxycarbonylamino-cyclohexyl)-methan (h mdu) wurden als schmelze (140 °c) in die wälzung des fallfilmverdampfers der spalt- und rektifizierkolonne gefahren, wobei die deblockierungsreaktion bei einer temperatur von 237 °c und einem sumpfdruck von 10 mbar in gegenwart einer stationären konzentration an zinndichlorid von 18 ppm durchgeführt wurde.
the remaining 628.7 g/h of bis(4-butoxycarbonylaminocyclohexyl)methane (h mdu) were conducted as a melt (140° c.) into the circulation of the falling-film evaporator of the cleavage and rectification column, and the deblocking reaction was carried out at a temperature of 237° c. and a bottom pressure of 10 mbar in the presence of a steady-state concentration of tin dichloride of 18 ppm.
Última atualização: 2014-12-03
Frequência de uso: 4
Qualidade: