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bifle
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2-3 détermination de la masse du peptide natif, du peptide s-pyridyléthylé et des fragments de protéolyse .par spectrométrie de masse maldi-tof (matrix assisted laser desorption ionization-time of flight). les mesures de masses ont été effectuées sur un spectromètre de masse maldi- tof bruker biflex (bremen, allemagne) en mode linéaire positif.
2-3 determination of the mass of the native peptide, of the s-pyridylethylated peptide and of the proteolysis fragments by maldi-tof (matrix assisted laser desorption ionization-time of flight) mass spectrometry the mass measurements were carried out on a bruker biflex maldi-tof mass spectrometer (bremen, germany) in a positive linear mode.