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t eb = 92-95 °c (liquide incolore).
t eb =92-95° c. (colourless liquid).
Last Update: 2014-12-03
Usage Frequency: 1
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après 30 minutes d'agitation, la température ayant évolué jusqu'à température ambiante, on verse le mélange réactionnel dans de l'eau glacée, extrait avec de l'acétate d'éthyle, sèche et évapore à sec sous pression réduite. on obtient 38,5 g du produit attendu sous forme d'une huile (t eb : 230°c sous 10 -2 mbar) rf : 0,36 (chromatographie sur couche mince, support : silice, éluant cyclohexane).
after stirring for 30 minutes with the temperature having risen to ambient temperature, the reaction mixture was poured into ice-cooled water and extraction was carried out with ethyl acetate, followed by drying and evaporating to dryness under reduced pressure to obtain 38.5 g of the expected product in the form of an oil (t.sub.eb : 230 layer chromatography, support: silica, eluant: cyclohexane).
Last Update: 2014-12-03
Usage Frequency: 1
Quality:
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