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con agua, transvasar el líquido a un frasco aforado de 250 ml despreciando el hierro no disuelto. enrasar con agua.
with water, quantitatively transfer the liquid into a 250-ml graduated flask, leaving behind the undissolved iron - make up to the mark with the water.
dejar refrigerar, transvasar la solución en un matraz aforado de 1 l, completar el volumen con agua, homogeneizar y filtrar .
leave to cool, transfer the solution to a 1 litre graduated flask, make up to volume with water, homogenize and filter .
transvasar cuantitativamente a un matraz aforado de 50 ml, enrasar con solución reguladora de citrato (3.24) y mezclar.
transfer quantitatively to a 50 ml graduated flask and make up to the mark with citrate buffer (3.24) and mix.
disolver nuevamente el residuo en 3-4 ml de fase móvil (3.8) y transvasar cuantitativamente a un matraz aforado de 10 ml.
re-dissolve the residue in 3 to 4 ml of mobile phase (3.8) and transfer quantitatively to a 10 ml graduated flask.
transvasar 0,5, 1,0 y 2,0 ml de la solución patrón intermedia (3.7.2) a una serie de matraces aforados de 50 ml.
transfer 0,5, 1,0 and 2,0 ml of the intermediate standard solution (3.7.2) into a series of 50 ml graduated flasks.
transvasar 10,0 ml de la solución patrón madre (3.5.1) a un matraz aforado de 100 ml, enrasar con la fase móvil (3.4) y mezclar.
transfer 10,0 ml of the stock standard solution (3.5.1) into a 100 ml graduated flask, make up to the mark with the mobile phase (3.4) and mix.