You searched for: laufmittelgemische (Tyska - Engelska)

man erhielt 3,69 g (99% der theorie) der titelverbindung als farblose kristalle. r = 0,67, laufmittelgemisch iv ms (dci, nh₃): m/z = 148 (m+h)⁺ (s)-2-amino-1-cyclohexylbut-3-en hydrochlorid wie für beispiel i beschrieben erhielt man aus 5.07 g (20,00 mmol) (s)-2-(tert.butoxycarbonylamino-1-cyclohexylbut-3-en [j.r. luly et al., j. org. chem. , 1487 (1987)] 3,76 g (99% der theorie) der titelverbindung als farblose kristalle.
3.69 g (99% of theory) of the title compound were obtained as colourless crystals. r.sub.f =0.67, eluent mixture iv ms (dci, nh.sub.3): m/e=148 (m+h).sup.+ example ii (s)-2-amino-1-cyclohexylbut-3-ene hydrochloride ##str64## as described for example i, 3.76 g (99% of theory) of the title compound were obtained as colourless crystals from 5.07 g (20.00 mmol) of (s)-2-(tert-butoxycarbonylamino-1-cyclohexylbut-3-ene [j. r. luly et al., j. org. chem. 52, 1487 (1987)].