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procédé selon la revendication 5 , caractérisé en ce que le catalyseur est le bromure de tributylhexadécylphosphonium ou le bromure de tétrabutylphosphonium.
process according to claim 5, characterized in that the catalyst is tributylhexadecylphosphonium bromide or tetrabutylphosphonium bromide.
Last Update: 2014-12-04
Usage Frequency: 2
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b ) catalyse par le bromure de tributylhexadécylphosphonium . on agite un mélange de 1,73 g ( 13 mmol) d'anisonitrile avec 2,07 g ( 14,7 mmol) de chlorure de benzoyle et 0,33 g (0,65 mmol, 0,05 éq ) de bromure de tributylhexadécylphosphonium à 185°c pendant 16 heures .
b. catalysis by tributylhexadecylphosphonium bromide a mixture of 1.73 g (13 mmol) of anisonitrile with 2.07 g (14.7 mmol) of benzoyl chloride and 0.33 g (0.65 mmol, 0.05 eq.) of tributylhexadecylphosphonium bromide is stirred at 185 hours.
Last Update: 2014-12-03
Usage Frequency: 1
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