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the xrd pattern shows two strong distinct refection peaks appearing at 2θ=21.36° and 2θ=23.69° along with a peak at 2θ=35.92° corresponding to the inter planner spacing of 4.132, 3.707 and 2.481 a˚, respectively. the three peaks correspond to the orthorhombic crystallite lattice planes. this the xrd pattern shows two strong distinct refection peaks appearing at 2θ=21.36° and 2θ=23.69° along with a peak at 2θ=35.92° corresponding to the inter planner spacing of 4.132, 3.707 and 2.481 a˚, respectively. the three peaks correspond to the orthorhombic crystallite lattice planes (110), (200) and (020). this indicates that hdpe used in this investigation has orthorhombic structure. another moderately strong peak appears at 2θ=30.68° corresponds to (210) plane. moreover, other small peaks appear at angles 2θ>40° indicating the semicrystalline nature of hdpe (i.e., presence of crystalline and amorphous regions). this xrd pattern demonstrates that hdpe used in this study is pure and without any impurities [66]. with irradiation, peak intensities corresponding to the (110), (200) planes increased. this could be explained by the fact that gamma irradiation generally results in chain splitting that is stimulated by oxidative reaction in amorphous regions. this contributes to the formation of crystallites in the amorphous region as free radicals are produced. free radicals appear to crosslink with other polymer chains resulting in increased crystallinity
jalur beberapa puncak yang ditunjukkan dalam spektrum ftir terhasil daripada kemerosotan oksidatif akibat penyinaran gamma muncul dalam julat 875-1370 cm-1. band ini mungkin disebabkan oleh regangan co dan lenturan oh. satu lagi puncak tambahan menunjukkan penyinaran sekitar 1720 cm-1. puncak ini dilaporkan oleh ramai penyelidik dan ia sepadan dengan ikatan co yang meregangkan dalam kumpulan karbonil yang terbentuk akibat pengoksidaan juga. akhirnya, puncak baru dapat dilihat sekitar 3680 cm-1; puncak ini mungkin atribut